how are nanomaterials prepared by ball milling and sol gel method

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    Dec 08, 2017· In this video, i have discussed the principle, procedure, reaction mechanism involved in the SOL GEL method, used for the synthesis of nano metal oxide.

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  • Sol gel synthesis of nanoparticles - SlideShare

    Dec 01, 2014· Sol-gel Processing The sol-gel process is a wet-chemical technique that uses either a chemical solution (sol short for solution) or colloidal particles (sol for nanoscale particle) to produce an integrated network (gel). Metal alkoxides and metal chlorides are typical precursors.

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    1.2 Method of synthesis There are five widely known methods of production of nanomaterials they are given as follows: Sol-gel synthesis. Inert gas condensation. Mechanical alloying or high-energy ball milling. Plasma synthesis. Electrodeposition. 1.2.1 Sol-Gel Synthesis:

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    The silver/silica nanocomposites have been successfully prepared by the sol-gel process. After drying in air at 70°C for 30 min, samples are heat treated in air at 150, 300 and 500°C.

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    The various as-prepared (Zn(1-x)Cu(x))O materials were analyzed by powder X-ray diffraction (pXRD), FT-IR, and SEM-EDX measurements in order to check the phase formation, purity, surface morphology and elements present in the annealed materials. Due to the preparation methods as well as doping of 'x' slight variations in cell parameters are seen.

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    Sol–gel research grew to be so important that in the 1990s more than 35,000 papers were published worldwide on the process. Particles and polymers. The sol–gel process is a wet-chemical technique used for the fabrication of both glassy and ceramic materials.

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    Fig.1(c ) XRD patterns of zinc oxide nanoparticles (hydrothermal method) 3.2 Structural studies Fig. 2(a) shows that the SEM images of zinc oxide nanoparticles obtained by aqueous solution method.. The image shows spherical and flower like structure. Fig.2(b) shows SEM images of the ZnO nano powders prepared by sol-gel method.

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    3.1.9 Conventional Sol-Gel Method The sol-gel method is a versatile process used for synthesizing various oxide materials [29]. This synthetic method generally allows control of the texture, the chemical, and the morphological properties of the solid. This method also has several advantages

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    Apr 29, 2011· In this new method a magnet is placed close to the cell to apply a strong magnetic pulling force on the magnetic milling balls, and therefore the impact energy is much higher than the conventional ball milling energy.